HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 22600667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | HCID 18997705 | HCID 18997705 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22600667 | HCID 22600667 | — |
Reaction Steps
The suspension obtained on mixing 150 ml of 96° strength ethanol, 16 ml of water, 2.3 g of ammonium chloride and 78 g of finely powdered zinc is brought to reflux. 25.1 g (0.15 mol) of 2-methylthio-5-nitrophenol are added portionwise so as to maintain the reflux without heating (exothermic reaction).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478359 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-0270df3376064a2eaafaf9ff24fb5efd |
| Source note | uspto-grants-1995_12 |