HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trimethoxyaniline → 2-Methyl-6,11-dihydro-dibenzo[b,e]oxepine-11-carboxylic acid (2,4,6-trimethoxy-phenyl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trimethoxyaniline | HCID 84271 | — |
| Reactant | 6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid | HCID 10106342 | — |
| Product | 2-Methyl-6,11-dihydro-dibenzo[b,e]oxepine-11-carboxylic acid (2,4,6-trimethoxy-phenyl)-amide | HCID 10251504 | 40.8% |
Reaction Steps
The similar procedures as in Example 1 were repeated except using 2.32 g of Compound A and 1.85 g of 2,4,6-trimethoxyaniline in place of aniline to obtain 1.56 g of Compound 10 as amorphous.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478835 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-146c41e9e9ca4133b33ef2ff25291a5f |
| Source note | uspto-grants-1995_12 |