HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Diethylaniline → Dibenz(b,e)oxepin-11-carboxamide, 6,11-dihydro-2-bromo-N-(2,6-diethylphenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Diethylaniline | HCID 11369 | — |
| Reactant | 2-Bromo-6,11-dihydrodibenz[b,e]oxepin-11-carboxylic acid | HCID 10403641 | — |
| Product | Dibenz(b,e)oxepin-11-carboxamide, 6,11-dihydro-2-bromo-N-(2,6-diethylphenyl)- | HCID 3072814 | 64% |
Reaction Steps
The similar procedures as in Example 1 were repeated except using 1.37 g of Compound H obtained in Example 46 in place of Compound A and 0.59 g of 2,6-diethylaniline in place of aniline to obtain 1.14 g of Compound 27.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478835 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-e448cdd0264e4cd7a76c64c54fd15140 |
| Source note | uspto-grants-1995_12 |