Diisopropylaniline → 144170-21-8

HRID 2260587Notes

Reaction equation

HRID 2260587 reaction equation
[Br:1][C:2]1[CH:3]=[CH:4][C:5]2[CH:11]([C:12](O)=[O:13])[C:10]3[CH:15]=[CH:16][CH:17]=[CH:18][C:9]=3[CH2:8][O:7][C:6]=2[CH:19]=1.[CH:20]([C:23]1[CH:29]=[CH:28][CH:27]=[C:26]([CH:30]([CH3:32])[CH3:31])[C:24]=1[NH2:25])([CH3:22])[CH3:21]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]2[CH:11]([C:12]([NH:25][C:24]3[C:26]([CH:30]([CH3:31])[CH3:32])=[CH:27][CH:28]=[CH:29][C:23]=3[CH:20]([CH3:22])[CH3:21])=[O:13])[C:10]3[CH:15]=[CH:16][CH:17]=[CH:18][C:9]=3[CH2:8][O:7][C:6]=2[CH:19]=1

Participants

3

Reactant 2

HCID 32484DiisopropylanilineHCID 10381245HCID 10381245, compound

Product 1

HCID 3072816144170-21-8Yield 73.4%

Procedure

The similar procedures as in Example 1 were repeated except using 1.40 g of Compound K in place of Compound A and 0.78 g of 2,6-diisopropylaniline in place of aniline to obtain 1.54 g of Compound 29.

Sources & evidence

ORD record
ord-762406311f934df89fa030a2a750e0d3
Source dataset
uspto-grants-1995_12
Patent number
US05478835

Reaction notes

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