HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichloroaniline → 2-Bromo-N-(2,6-dichlorophenyl)-6,11-dihydrodibenz[b,e]oxepin-11-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichloroaniline | HCID 11846 | — |
| Reactant | 2-Bromo-6,11-dihydrodibenz[b,e]oxepin-11-carboxylic acid | HCID 10403641 | — |
| Product | 2-Bromo-N-(2,6-dichlorophenyl)-6,11-dihydrodibenz[b,e]oxepin-11-carboxamide | HCID 10367114 | 18.4% |
Reaction Steps
The similar procedures as in Example 1 were repeated except using 1.67 g of 2-bromo-6,11-dihydrodibenz[b,e]oxepin-11-carboxylic acid obtained in Example 46 (Compound H) in place of Compound A and 0.76 g of 2,6-dichloroaniline in place of aniline to obtain 0.40 g of Compound 39.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478835 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-89037247c01541faa79f50124641ead4 |
| Source note | uspto-grants-1995_12 |