HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 18998777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 4-(2-Chlorothiazol-5-yl)-4-methoxy-2,2-dimethyltetrahydropyran | HCID 18998778 | — |
| Reactant | 1-Methyl-6-sulfanyl-1,2,3,4-tetrahydroquinolin-2-one | HCID 22413759 | — |
| Product | HCID 18998777 | HCID 18998777 | 80% |
Reaction Steps
Using an analogous procedure to that described in Example 1 except that a catalytic amount (0.01 g) of potassium iodide was added, 6-mercapto-1-methyl-1,2,3,4-tetrahydroquinolin-2-one was reacted with 4-(2-chlorothiazol-5-yl)-4-methoxy-2,2-dimethyltetrahydropyran to give 4-methoxy-2,2-dimethyl-4-[2-(1-methyl-2-oxo-1,2,3,4-tetrahydroquinolin-6-ylthio)thiazol-5-yl]tetrahydropyran in 80% yield as a foam;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478843 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-4e574e22ff764758bbd5e024e42759d5 |
| Source note | uspto-grants-1995_12 |