HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 10703813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | 1,3-Benzodioxol-5-amine, N-methyl- | HCID 10606919 | — |
| Product | HCID 10703813 | HCID 10703813 | — |
Reaction Steps
By following the procedure described in example 1A N-methyl-3,4-methylenedioxyaniline (N. J. Houlihan et al., J.Het. Chem. 19, 1453 (1982)) (3.02 g, 20 mmol) was reacted with phosgene to give 3.0 g N-methyl-N -(3,4-methylenedioxyphenyl)carbamoylchloride. M.p. 71°-73° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478845 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-1ac5d37734da49a2accfd0b3d8b8881d |
| Source note | uspto-grants-1995_12 |