HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10703813, compound → HCID 131719231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10703813 | HCID 10703813 | — |
| Reactant | 3-(4-(6-Fluorobenzo[d]isoxazol-3-yl)piperidin-1-yl)propan-1-ol | HCID 15384966 | — |
| Product | HCID 131719231 | HCID 131719231 | 34.6% |
Reaction Steps
By following the procedure described in example 2B 3-(4-(6-fluoro -1,2-benzisoxazol-3-yl)piperidino)propanol (278 mg, 1 mmol) was reacted with N-methyl-N-(3,4-methylenedioxyphenyl)carbamoylchloride (240 mg, 1.12 mmol) to give 170 mg of the title compound. M.p. 126°-129° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478845 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-57437141a9de4cd6b0befe9b0b0de902 |
| Source note | uspto-grants-1995_12 |