HuagongsheHuagongshe Chemistry Print Report · For research reference only
5H-[1,3]dioxolo[4,5-f]indole → HCID 12369276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5H-[1,3]dioxolo[4,5-f]indole | HCID 260797 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12369276 | HCID 12369276 | 42.1% |
Reaction Steps
5,6-methylenedioxyindole (1.3 g, 8 mmol) dissolved in 25 ml glacial acetic acid was reduced catalytically (1 atm., 22° C.) using 370 mg PtO2 hydrate to give 550 mg of crude 2,3-dihydro-5,6-methylenedioxyindole which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478845 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-8205f5b58f0d4888ac07ad44c2f92e72 |
| Source note | uspto-grants-1995_12 |