HCID 57111979, compound → HCID 18998903, compound

Participants

Reaction Steps

A mixture of 4-[2-(2,3-dihydro-1H-isoindol-1-on-2-yl)-ethoxy]benzyl alcohol (2.97 g), manganese(IV) oxide (9.12 g) and dichloromethane (180 ml) was stirred for 3 hours at room temperature. The mixture was filtered through a Soxhlet thimble and the residue extracted with refluxing dichloromethane for 3 hours. The solvent was then evaporated to afford the title compound, mp 134°-135° C.

Provenance & Evidence