Octyl isocyanate → HCID 131728562, 화합물

HRID 2261182노트

반응식

HRID 2261182 반응식
[O:1]1[C:9]2[C:4](=[N:5][CH:6]=[CH:7][CH:8]=2)[NH:3][C:2]1=[O:10].N([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])=C=O>O1CCOCC1>[O:10]=[C:2]1[NH:3][C:4]2=[N:5][CH:6]=[CH:7][CH:8]=[C:9]2[O:1]1.[CH3:21][CH2:20][CH:19]([C:2]([NH2:3])=[O:1])[CH2:18][CH2:17][CH2:16][CH2:15][CH3:14]

참가 물질

4

반응물 2

HCID 76616Octyl isocyanateHCID 2799900Oxazolo(4,5-b)pyridin-2(3H)-one

생성물 1

HCID 131728562HCID 131728562, 화합물

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

200 mg (1.47 mmol) of 3H-oxazolo[4,5-b]pyridin-2-one were reacted in analogy to Example 1 with 273.7 mg (1.76 mmol) of 1-isocyanatooctane in dioxane at 80° C. Yield: 40 mg (9%), M+H+: 292.10.

출처 및 근거

ORD 기록
ord-ab06005992dd4c0e86067dba01966af4
출처 데이터셋
uspto-grants-2010_12
특허 번호
US07846943B2

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