HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 86631049, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | 2-ethylthio-1-methylimidazole-5-carbaldehyde | HCID 2763310 | — |
| Product | HCID 86631049 | HCID 86631049 | — |
Reaction Steps
5.13 g of 2-ethylthio-1-methylimidazole-5-carbaldehyde was dissolved in 30 ml of ethanol, and 2.00 g of malononitrile was then added. The mixture was stirred at room temperature for 3 hours. The reaction mixture was concentrated under reduced pressure. The residue was subjected to silica gel column chromatography to obtain 2.51 g of [(2-ethylthio-1-methylimidazol-3-yl)methylidene]malononitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07846956B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-d071acc5f2a64e3d978898df9886a5ba |
| Source note | uspto-grants-2010_12 |