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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2261366Generated: November 3, 2026

Ethanol → HCID 86631049, compound

https://huagongshe.com/reaction/2261366

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantMalononitrileHCID 8010—
Reactant2-ethylthio-1-methylimidazole-5-carbaldehydeHCID 2763310—
ProductHCID 86631049HCID 86631049—

Reaction Steps

5.13 g of 2-ethylthio-1-methylimidazole-5-carbaldehyde was dissolved in 30 ml of ethanol, and 2.00 g of malononitrile was then added. The mixture was stirred at room temperature for 3 hours. The reaction mixture was concentrated under reduced pressure. The residue was subjected to silica gel column chromatography to obtain 2.51 g of [(2-ethylthio-1-methylimidazol-3-yl)methylidene]malononitrile.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07846956B2
Source datasetuspto-grants-2010_12
ORD IDord-d071acc5f2a64e3d978898df9886a5ba
Source noteuspto-grants-2010_12