HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → HCID 11406298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | O-Benzylhydroxylamine | HCID 102313 | — |
| Reactant | HCID 11219135 | HCID 11219135 | — |
| Product | HCID 11406298 | HCID 11406298 | 75% |
Reaction Steps
Benzyloxyamine was added to organic solvent dissolving 30 mg of 3-(1-benzyl-2-oxo-1,2,5,6-tetrahydro-pyridin-3-yl)-propionic acid (0.15 mmol) prepared by above Example 12 in EDC. The resulting compound was purified by Silica gel column chromatography with ethylacetate/chloroform (1:1) solvent mixture as an eluant to give 41 mg of the title compound (g5) (yield: 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07846963B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-cfea9ceb45f64acbaad18646f7e94af7 |
| Source note | uspto-grants-2010_12 |