HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 49845771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 2-[(Carboxymethyl)amino]pyridine-3-carboxylic acid | HCID 59593329 | — |
| Product | HCID 49845771 | HCID 49845771 | — |
Reaction Steps
Acetic acid 1-acetyl-1H-pyrrolo[2,3-b]pyridin-3-yl ester 502 is prepared by reacting 2-(Carboxymethyl-amino)-nicotinic acid 501 with sodium acetate in refluxing acetic anhydride for several hours, followed by purification and isolation by conventional means (e.g. recrystallization) (Su & Tsou; J. Am. Chem. Soc., 82, 1960, 1187).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07846941B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-73710bc60cc84dd789cabd0251b18bc1 |
| Source note | uspto-grants-2010_12 |