Hydrochloric Acid → HCID 68780482, compound
Reaction equation
ClC(CC)CC(C1C=CC=CC=1N)C.[CH2:15]1[CH2:17][CH:16]1[C:18]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=1[NH:27]C(=O)C(C)(C)C)([CH3:20])[CH3:19].Cl>>[CH2:15]1[CH2:17][CH:16]1[C:18]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=1[NH2:27])([CH3:20])[CH3:19]Participants
4
Procedure
2-(3-Chloro-1-methylpentyl)phenylamine (III-3) is obtained by initially preparing N-[2-(2-cyclopropylisopropyl)phenyl]-2,2-dimethylpropanamide analogously to Examples (III-1a) and (III-1b). In the third step, the material is reacted with hydrochloric acid which gives, in addition to 2-(2-cyclopropylisopropyl)phenylamine, also the compound (III-3).
Sources & evidence
- ORD record
- ord-96e00bc829d243c5ad8171040495e733
- Source dataset
- uspto-grants-2010_12
- Patent number
- US07847108B2
Reaction notes
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