Gamma-Butyrolactone → HCID 20542950, compound

HRID 2261722Notes

Reaction equation

HRID 2261722 reaction equation
[CH2:1]([NH2:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:10]1(=[O:15])[O:14][CH2:13][CH2:12][CH2:11]1>>[CH2:1]([NH:9][C:13](=[O:14])[CH2:12][CH2:11][CH2:10][OH:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 7302Gamma-ButyrolactoneHCID 8143Octylamine

Product 1

HCID 20542950HCID 20542950, compound

Procedure

1 mol of octylamine was heated to 100° C. with stirring. 1 mol of gamma-butyrolactone was added dropwise over a period of 30 minutes. The mixture was heated for three hours to 120° C. At the end of the reaction, a vacuum of 50 mbar was applied. The product was obtained after cooling in the form of a pale yellow solid.

Workup

  1. temperatureThe mixture was heated for three hours to 120° C
  2. customAt the end of the reaction
  3. customThe product was obtained
  4. temperatureafter cooling in the form of a pale yellow solid

Sources & evidence

ORD record
ord-e207e4cce8a64cc29267cb186d6abf28
Source dataset
uspto-grants-2010_12
Patent number
US07847123B2

Reaction notes

Loading…