HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-methoxy-2-methylbenzoate → Methyl 4-hydroxy-2-methylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-methoxy-2-methylbenzoate | HCID 13257269 | — |
| Reactant | HCID 57443304 | HCID 57443304 | — |
| Product | Methyl 4-hydroxy-2-methylbenzoate | HCID 12351986 | 77% |
Reaction Steps
The title compound (77%) is prepared essentially according to the preparation of 5-hydroxy-2-propyl-benzoic acid methyl ester using 4-methoxy-2-methyl-benzoic acid methyl ester. 1H NMR (400 MHz, CDCl3) δ 7.91-7.86 (m, 1H), 6.72-6.67 (m, 2H), 3.86 (s, 3H), 2.57 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07846960B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-4dc682541de245f98e0ec8773c14bce9 |
| Source note | uspto-grants-2010_12 |