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HRID2262049

反应详情

EQUATION

反应方程式

HRID 2262049 的结构方程式

REACTANTS

反应物

2
结构：CN1CCNCC1
HCID53167

1-Methylpiperazine

C5H12N2

结构：O=C(O)c1cc2c(N3CCOCC3)nc(-c3cccc4[nH]ncc34)nc2s1
HCID59592885

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCN(C(=O)c2cc3c(N4CCOCC4)nc(-c4cccc5[nH]ncc45)nc3s2)CC1
HCID59592935

未命名化合物

PROCEDURE

实验过程

45 mg of 2-(1H-indazol-4-yl)-4-morpholinothieno[2,3-d]pyrimidine-6-carboxylic acid 14 was coupled to 1-methylpiperazine via General Procedure B. The product was purified via reverse phase HPLC to give 34.5 mg of 122. MS (Q1) 464.2 (M)+.

WORKUP

后处理

  1. customThe product was purified via reverse phase HPLC