HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 6-chloropyridine-3-carboxylate → HCID 25132124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 6-chloropyridine-3-carboxylate | HCID 254249 | — |
| Reactant | HCID 178506308 | HCID 178506308 | — |
| Product | HCID 25132124 | HCID 25132124 | 76% |
Reaction Steps
As described for Example 4, 4-(1H-imidazol-4-yl)-3-phenyl-5-trifluoromethyl-isoxazole (450 mg, 0.1.6 mmol) was converted, using methyl 6-chloronicotinate instead of 4-fluorobenzotrifluoride, to the title compound (510 mg, 76%) which was obtained as a white solid. MS: m/e=415.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07851469B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-4610ecee8d7a41f8b7ecf8f939ec499f |
| Source note | uspto-grants-2010_12 |