Ammonium Hydroxide → HCID 68685144, compound

Participants

Reaction Steps

[2-Acetylamino-5-(4-methyl-piperazin-1-yl)-phenyl]-acetic acid ethyl ester (450 mg, 1.41 mmol) is suspended in a 33% aqueous NH4OH solution (200 mL), and stirred for 16 h at RT. The volume is carefully reduced under vacuum until the title compound remains as a brown solid, which is further dried under high vacuum. ES+-MS: 291 [M+H]+.

Provenance & Evidence