HCID 68686602, compound → HCID 68689964, compound

Participants

Reaction Steps

To a solution of [5-(4-Methyl-piperazin-1-yl)-2-nitro-phenyl]-acetic acid ethyl ester (1.10 g, 3.58 mmol) in MeOH (25.0 mL) is added 10% Pd on charcoal (114 mg). The reaction mixture is stirred for 4 h under a hydrogen atmosphere (1 atm.), filtered through a microfilter (0.45 μM), and the filtrate concentrated at reduced pressure to afford the title compound as a red oil. ES+-MS: 278 [M+H]+.

Provenance & Evidence