HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57442328, compound → HCID 57442329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57442328 | HCID 57442328 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57442329 | HCID 57442329 | — |
Reaction Steps
Dissolve benzyl 4-(4-acetylphenyl)-3-oxopiperazine-1-carboxylate (420 mg, 1.20 mmol) in MeOH (100 mL). Flush the flask with N2 and add 10% Pd/C (100 mg). Hydrogenate overnight under a hydrogen filled balloon. Remove the catalyst by filtration through Celite and wash with MeOH. Evaporate the solvent to yield the title compound. LC-MS (M+1): 219.13.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07851474B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-089316c00ef84c358bb548ae6d89ab06 |
| Source note | uspto-grants-2010_12 |