HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 11630692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 57438788 | HCID 57438788 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11630692 | HCID 11630692 | — |
Reaction Steps
Preparation according to Example 8: 4-[2-fluoro-3-(trifluoromethoxy)phenyl]piperidine (0.70 g, 2.66 mmol), acetonitrile (4 ml), potassium carbonate (0.92 g, 6.65 mmol), 1-iodoethane (0.275 ml, 2.93 mmol). Yield: 0.7 g. MS m/z (rel. intensity, 70 eV) 291 (M+, 14), 290 (10), 277 (15), 276 (bp), 193 (8).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07851629B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-6da9c761e25845dba38514f5e9256eb7 |
| Source note | uspto-grants-2010_12 |