HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopropane → HCID 68778013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 17898951 | HCID 17898951 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68778013 | HCID 68778013 | — |
Reaction Steps
Preparation according to preparation 10: 4-(2,3-dichlorophenyl)pyridine (1.0 g, 4.46 mmol), 1-iodopropane (6 ml), ethanol (60 ml), sodium borohydride (1.5 g, 44 mmol). Yield: 0.45 g. MS m/z (rel. intensity, 70 eV) 271 (M+, 16), 269 (M+, 28), 242 (62), 240 (bp), 127 (11).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07851629B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-689f230ce240418d9b5ea1a7b756464a |
| Source note | uspto-grants-2010_12 |