HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57438798, compound → HCID 57438799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57438798 | HCID 57438798 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57438799 | HCID 57438799 | — |
Reaction Steps
According to Preparation 4: Tert-butyl-4-(2,3-dichlorophenyl)-4-hydroxypiperidine-1-carboxylate (3.0 g, 8.7 mmol), trifluoroacetic acid (30 ml). Yield: 0.88 g. MS m/z (rel. intensity, 70 eV) 229 (63), 228 (M+, 36), 227 (bp), 163 (53), 82 (85).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07851629B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-49a13a162cb24e56aeea842a327b3351 |
| Source note | uspto-grants-2010_12 |