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HRID22638

反应详情

EQUATION

反应方程式

HRID 22638 的结构方程式

REACTANTS

反应物

2
结构：O=C=Nc1ccc(I)cc1
HCID3399787

4-Iodophenyl isocyanate

C7H4INO

结构：CCCNN(C(=O)OC(C)(C)C)c1cccc(C#N)c1
HCID22591495

未命名化合物

PRODUCTS

生成物

1
结构：CCCN(C(=O)Nc1ccc(I)cc1)N(C(=O)OC(C)(C)C)c1cccc(C#N)c1
HCID11191609

未命名化合物

收率 84.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

2.0 g (7.273 mmol) of 404 are stirred at RT for 1.5 h in 5.0 ml of pyridine with 1.78 g (7.265 mmol) of 4-iodophenyl isocyanate. After customary work-up, 3.2 g (84.7%) of 405 are thus obtained as crystals having a melting point of 184-185° C.; MS(FAB)=521.