HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodo-4-isocyanatobenzene → tert-Butyl 2-(3-cyanophenyl)-3-(4-iodophenylaminocarbonyl)-3-propylcarbazate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodo-4-isocyanatobenzene | HCID 3399787 | — |
| Reactant | tert-Butyl 2-(3-cyanophenyl)-3-propylcarbazate | HCID 22591495 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | tert-Butyl 2-(3-cyanophenyl)-3-(4-iodophenylaminocarbonyl)-3-propylcarbazate | HCID 11191609 | 84.7% |
Reaction Steps
2.0 g (7.273 mmol) of 404 are stirred at RT for 1.5 h in 5.0 ml of pyridine with 1.78 g (7.265 mmol) of 4-iodophenyl isocyanate. After customary work-up, 3.2 g (84.7%) of 405 are thus obtained as crystals having a melting point of 184-185° C.; MS(FAB)=521.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849626B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-b11fe237dcff4b788461ffd92d003266 |
| Source note | uspto-grants-2005_02 |