HRID22640

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCCN(C(=O)Nc1ccc(-c2ccccc2S(=O)(=O)NC(C)(C)C)cc1)N(C(=O)OC(C)(C)C)c1cccc(C(=N)N)c1

HCID11157869

未命名化合物

PRODUCTS

生成物

结构：CCCN(Nc1cccc(C(=N)N)c1)C(=O)Nc1ccc(-c2ccccc2S(N)(=O)=O)cc1

HCID9847374

未命名化合物

收率 99.3%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6422

未命名化合物

PROCEDURE

实验过程

0.5 g (0.803 mmol) of 408 is dissolved in 5.0 ml of trifluoroacetic acid and stirred at 5C for 18 h. After customary work-up, 0.15 g (99.3%) of 1 is thus obtained as crystals having a melting point of 215-216° C.; MS(FAB)=467.