HCID 59595974, compound → HCID 59595979, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of 5′-nitro-4,2′:3′,4″-terpyridin-6′-amine (0.144 g, 0.490 mmol) in ethanol (5 mL), 0.300 mL of hydrogen chloride and 0.140 g (2.45 mmol) of iron were added. The mixture was heated at 90° C. for 2 h and the solvent was evaporated. The crude mixture was extracted between ethyl acetate and water. The organic layer was dried (MgSO4) and the solvent evaporated to give the title compound (0.120 g, 93% of yield).

Provenance & Evidence