HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloro-3-nitropyridin-2-ylamine → 3'-Chloro-5-nitro-2,4'-bipyridin-6-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloro-3-nitropyridin-2-ylamine | HCID 2724035 | — |
| Reactant | 3-Chloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine | HCID 44755154 | — |
| Product | 3'-Chloro-5-nitro-2,4'-bipyridin-6-amine | HCID 59596017 | 99% |
Reaction Steps
Following the same procedure as in Intermediate 1 (step a), but using 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-chloropyridine, 6-chloro-3-nitropyridin-2-amine was transformed into the title compound as a white solid (2.14 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855202B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-6b4fce7954d64b9b8209d045f16683d0 |
| Source note | uspto-grants-2010_12 |