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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2264188Generated: October 31, 2026

Ammonia → HCID 59595967, compound

https://huagongshe.com/reaction/2264188

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantHCID 59595975HCID 59595975—
ProductHCID 59595967HCID 5959596777%

Reaction Conditions

Temperature100 °C

Reaction Steps

A suspension of 2-methoxy-3-nitro-6-(1,3-oxazol-2-yl)pyridine (0.187 g, 0.85 mmol) in aqueous ammonia (32%, 5 mL) was heated in a sealed tube to 100° C. with stirring. After 2.5 hours the mixture was cooled and the precipitate was filtered and washed with water and then dried in vacuo to give the title compound (0.134 g, 77%) as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07855202B2
Source datasetuspto-grants-2010_12
ORD IDord-bade95ccfb0740ec8e7645ffadde844b
Source noteuspto-grants-2010_12