Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 59595975 | HCID 59595975 | — |
| Product | HCID 59595967 | HCID 59595967 | 77% |
Reaction Steps
A suspension of 2-methoxy-3-nitro-6-(1,3-oxazol-2-yl)pyridine (0.187 g, 0.85 mmol) in aqueous ammonia (32%, 5 mL) was heated in a sealed tube to 100° C. with stirring. After 2.5 hours the mixture was cooled and the precipitate was filtered and washed with water and then dried in vacuo to give the title compound (0.134 g, 77%) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07855202B2 |
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| Source dataset | uspto-grants-2010_12 |
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| ORD ID | ord-bade95ccfb0740ec8e7645ffadde844b |
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| Source note | uspto-grants-2010_12 |
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