HCID 68790181, compound → HCID 178524347, compound

Participants

Reaction Steps

A solution of 4-[2-(6′-Amino-3″-fluoro-[3,2′;3′,4″]terpyridin-5′-ylcarbamoyl)-ethyl]-benzoic acid tert-butyl ester (0.135 g, 0.263 mmol) in acetic acid (2 mL) was heated in a sealed tube at 118° C. for 16 h. The solvent was evaporated and ethyl acetate was added. The solid formed was filtered and washed with 4% sodium bicarbonate aqueous solution, water and dried to give the title compound (0.08 g, 69% of yield).

Provenance & Evidence