Aniline → HCID 16742558, compound

Participants

Reaction Steps

Using the procedure of example 1, aniline (83 mg) was reacted with compound 1f (100 mg) to provide compound 3 (36 mg, 47%). 1H NMR (400 MHz, CD3OD) δ 8.88 (d, J=7.8 Hz, 1H), 8.29 (t, J=6.0 Hz, 2H), 8.19 (s, 1H), 7.69 (d, J=7.8 Hz, 2H), 7.36 (t, J=7.6 Hz, 2H), 7.21 (m, 1H), 7.08 (t, J=7.8 Hz, 2H). MS (ESI) m/z: 288 (M+H)+.

Provenance & Evidence