Cycloheptylamine → HCID 58692202, compound

Participants

Reaction Steps

Using the procedure of example 1, cycloheptylamine (92 mg) was reacted with compound 1f (100 mg) to provide compound 15 (34 mg, 41%). 1H NMR (400 MHz, CD3OD) δ 8.95 (d, J=8.0 Hz, 1H), 8.28 (d, J=4.8 Hz, 1H), 8.19 (s, 1H), 8.12 (d, J=5.6 Hz, 1H), 7.25 (dd, J=8.0 Hz, 4.8 Hz, 1H), 7.01 (d, J=5.6 Hz, 1H), 4.12 (m, 1H), 2.13 (m, 2H), 1.79-1.63 (m, 10H). MS (ESI) m/z: 308 (M+H)+.

Provenance & Evidence