2-Ethylaniline → HCID 44416063, compound

Participants

Reaction Steps

Using the procedure of example 1, 2-ethylaniline (98 mg) was reacted with compound 1f (100 mg) to provide compound 32 (44 mg, 52%). 1H NMR (400 MHz, CD3OD) δ 8.48 (d, J=8.0 Hz, 1H), 8.21-8.18 (m, 3H), 7.51 (d, J=7.2 Hz, 1H), 7.35 (d, J=7.2 Hz, 1H), 7.27 (m, 2H), 7.14 (d, J=5.2 Hz, 1H), 7.03 (dd, J=8.0 Hz, 4.8 Hz, 1H), 2.71 (q, J=7.6 Hz, 2H), 1.20 (t, J=7.6 Hz, 3H). MS (ESI) m/z: 316 (M+H)+.

Provenance & Evidence