反应详情

9-Methyl-3,9-diaza-bicyclo[3.3.1]nonane (2.0 g, 14.3 mmol), 5-(4-nitro-phenyl)-furan-2-carboxylic acid chloride (3.59 g, 14.3 mmol) and 1,2-dimethoxyethane (40 ml) was stirred at room temperature for 15 hours. The product was filtered and was purified by washing with 1,2-dimethoxyethane (100 ml). Yield 5.24 g (94%). Mp. 263° C.

1. filtrationThe product was filtered
2. customwas purified
3. washby washing with 1,2-dimethoxyethane (100 ml)