HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-Methyl-3,9-diazabicyclo[3.3.1]nonane → HCID 68647616, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-Methyl-3,9-diazabicyclo[3.3.1]nonane | HCID 18911 | — |
| Reactant | 5-(4-nitrophenyl)furan-2-carbonyl Chloride | HCID 3829983 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 68647616 | HCID 68647616 | — |
Reaction Steps
9-Methyl-3,9-diaza-bicyclo[3.3.1]nonane (2.0 g, 14.3 mmol), 5-(4-nitro-phenyl)-furan-2-carboxylic acid chloride (3.59 g, 14.3 mmol) and 1,2-dimethoxyethane (40 ml) was stirred at room temperature for 15 hours. The product was filtered and was purified by washing with 1,2-dimethoxyethane (100 ml). Yield 5.24 g (94%). Mp. 263° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855208B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-278b2934e4d1495a918b5a06a807af14 |
| Source note | uspto-grants-2010_12 |