Hydrochloric Acid → HCID 23112258, compound

HRID 2264330Notes

Reaction equation

HRID 2264330 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:9]=[CH:10][C:11]=1[CH:12](O)[CH:13]([CH3:18])[C:14](OC)=[O:15])[C:5]([O:7][CH3:8])=[O:6].Cl>O1CCOCC1>[CH3:18][C:13]1[C:14](=[O:15])[NH:1][C:2]2[C:11]([CH:12]=1)=[CH:10][CH:9]=[C:4]([C:5]([O:7][CH3:8])=[O:6])[CH:3]=2

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 23112270Methyl 2-amino-β-hydroxy-4-(methoxycarbonyl)-α-methylbenzenepropanoate

Product 1

HCID 23112258HCID 23112258, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Methyl 3-amino-4-(1-hydroxy-3-methoxy-2-methyl-3-oxopropyl)benzoate was treated with hydrochloric acid in 1,4-dioxane to obtain methyl 3-methyl-2-oxo-1,2-dihydroquinolin-7-carboxylate.

Sources & evidence

ORD record
ord-431c7bfb9b6144f59271d360b828890b
Source dataset
uspto-grants-2010_12
Patent number
US07855198B2

Reaction notes

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