HCID 59376682, compound → HCID 68646516, compound

Participants

Reaction Steps

Stir a mixture of 6-amino-2-methyl-3′,6′-dihydro-2′H-[3,4′]bipyridinyl-1′-carboxylic acid tert-butyl ester (2.12 g) and palladium on carbon 10% wet (330 mg) in methanol (29.30 mL) under H2 (45 psi) for 48 h. Filtered over a celite pad and remove the solvent under vacuum to afford 2.07 g of the title compound. MS (ES+): m/z=292 (M+H)+.

Provenance & Evidence