HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 136339049, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | ethyl 5-formyl-2-methyl-1h-pyrrole-3-carboxylate | HCID 255661 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 136339049 | HCID 136339049 | — |
Reaction Steps
To a solution of 5-formyl-2-methyl-1H-pyrrole-3-carboxylic acid ethyl ester (6.30 g, 0.034 mol) in EtOH (6.3 mL) was added a solution of hydrazine (1.69 mL, 0.034 mol). The reaction mixture was stirred at RT overnight. The resulting precipitate was filtered and dried in vacuo to give the titled compound, 6.79 g as a light yellow solid. This material was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855288B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-67d28d0de2f54c36a9a311e0ccb97d94 |
| Source note | uspto-grants-2010_12 |