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HRID2264860

反应详情

EQUATION

反应方程式

HRID 2264860 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccncc1
HCID7963

4-Methylpyridine

C6H7N

结构：CC(=O)OCCCCI
HCID2733405

4-Iodobutyl acetate

C6H11IO2

PRODUCTS

生成物

1
结构：CC(=O)OCCCC[n+]1ccc(C)cc1.[I-]
HCID68781463

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

10 mmol (0.93 g) γ-picoline and 10 mmol (2.42 g) 4-iodobutylacetate are heated 4 h at 120° C. and after cooling repeatedly stirred with ether, decanted a finally dried in vacuum.

WORKUP

后处理

  1. temperatureafter cooling repeatedly
  2. customdecanted
  3. customa finally dried in vacuum