HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylpyridine → 1-(4-Acetoxybutyl)-4-methyl-pyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylpyridine | HCID 7963 | — |
| Reactant | 4-Iodobutyl acetate | HCID 2733405 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1-(4-Acetoxybutyl)-4-methyl-pyridinium iodide | HCID 68781463 | — |
Reaction Steps
10 mmol (0.93 g) γ-picoline and 10 mmol (2.42 g) 4-iodobutylacetate are heated 4 h at 120° C. and after cooling repeatedly stirred with ether, decanted a finally dried in vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855293B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-a7c4bc6d527b4e8d97a03b4f193d3b19 |
| Source note | uspto-grants-2010_12 |