HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 46224840, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 59597173 | HCID 59597173 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 46224840 | HCID 46224840 | — |
Reaction Steps
To a solution of 6-methyl-1-(3-hydroxyphenyl)-1,2,3,4-tetrahydro-beta-carboline (1 equiv) in THF was added Et3N (2.2 equiv) and acetic anhydride (1.2 equiv). After one hour, the solution was purified by prep-HPLC to give 3-(2-acetyl-6-methyl-2,3,4,9-tetrahydro-1H-beta-carbolin-1-yl)phenol 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855295B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-9a6a9963720944cf988097d9be83bf1d |
| Source note | uspto-grants-2010_12 |