HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Hydrochloric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 59597144 | HCID 59597144 | — |
| Product | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 46225271 | HCID 46225271 | — |
Reaction Steps
(tert-Butoxy)-N-{2-[1-(3-hydroxyphenyl)-6-methyl-(1,2,3,4-tetrahydro-beta-carbolin-2-yl)]-2-oxoethyl}carboxamide 11 was treated with HCl in dioxane (4 N, 10 equiv) for 30 min, and the solvent was removed to give 3-(2-glycyl-6-methyl-2,3,4,9-tetrahydro-1H-beta-carbolin-1-yl)phenol 14 as its HCl salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855295B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-03cae3a3fa1f424cb23e10d2e885a45f |
| Source note | uspto-grants-2010_12 |