HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11337670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 59597095 | HCID 59597095 | — |
| Product | HCID 11337670 | HCID 11337670 | — |
Reaction Steps
(tert-Butoxy)-N-{3-[1-(3-hydroxyphenyl)-6-chloro-(1,2,3,4-tetrahydro-beta-carbolin-2-yl)]-3-oxopropyl}carboxamide was treated with HCl in dioxane (4 N, 10 equiv) for 30 min, and the solvent was removed to give a residue which was purified to yield 3-(2-beta-alanyl-6-chloro-2,3,4,9-tetrahydro-1H-beta-carbolin-1-yl)phenol 23.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855295B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-caa422c600144d49ae193482d3cbfdf3 |
| Source note | uspto-grants-2010_12 |