HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68486934, compound → HCID 25258034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68486934 | HCID 68486934 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 25258034 | HCID 25258034 | 80% |
Reaction Steps
Compound 3 (10 mg) was dissolved in methanol (1 ml), and a catalytic amount of palladium carbon was added thereto. The obtained mixture was stirred in a hydrogen atmosphere at room temperature for 5 hours. After the reaction was over, the reaction mixture was filtered through Celite, and the filtrate was purified by silica gel column chromatography to obtain Compound 4 (8 mg, 80%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855300B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-51c19b2a81de4c8a92cbe70b9b8e7947 |
| Source note | uspto-grants-2010_12 |