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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2265088Generated: October 29, 2026

HCID 68486934, compound → HCID 25258034, compound

https://huagongshe.com/reaction/2265088

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68486934HCID 68486934—
ReactantHCID 178418361HCID 178418361—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 25258034HCID 2525803480%

Reaction Steps

Compound 3 (10 mg) was dissolved in methanol (1 ml), and a catalytic amount of palladium carbon was added thereto. The obtained mixture was stirred in a hydrogen atmosphere at room temperature for 5 hours. After the reaction was over, the reaction mixture was filtered through Celite, and the filtrate was purified by silica gel column chromatography to obtain Compound 4 (8 mg, 80%) as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07855300B2
Source datasetuspto-grants-2010_12
ORD IDord-51c19b2a81de4c8a92cbe70b9b8e7947
Source noteuspto-grants-2010_12