HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 131728596, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | L-Tartaric acid | HCID 444305 | — |
| Reactant | HCID 68427262 | HCID 68427262 | — |
| Reactant | HCID 68427575 | HCID 68427575 | — |
| Product | HCID 131728596 | HCID 131728596 | — |
Reaction Steps
A free amine form of the entitled compound was obtained in the same manner as in Example 15, for which, however, (3R*,4R*)-4-o-tolyl-piperidin-3-ol obtained in Production Example 12 were used in place of (3S*,4S*)-4-o-tolyl-piperidin-3-ol used in Example 15. The obtained free amine compound and the same amount of L-tartaric acid were mixed in ethanol, and crystallized from heptane added thereto to obtain the entitled compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855294B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-4ce0392fe6b54029a3fd70e0b4596c40 |
| Source note | uspto-grants-2010_12 |