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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2265141Generated: November 1, 2026

Ethanol → HCID 131728596, compound

https://huagongshe.com/reaction/2265141

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantL-Tartaric acidHCID 444305—
ReactantHCID 68427262HCID 68427262—
ReactantHCID 68427575HCID 68427575—
ProductHCID 131728596HCID 131728596—

Reaction Steps

A free amine form of the entitled compound was obtained in the same manner as in Example 15, for which, however, (3R*,4R*)-4-o-tolyl-piperidin-3-ol obtained in Production Example 12 were used in place of (3S*,4S*)-4-o-tolyl-piperidin-3-ol used in Example 15. The obtained free amine compound and the same amount of L-tartaric acid were mixed in ethanol, and crystallized from heptane added thereto to obtain the entitled compound as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07855294B2
Source datasetuspto-grants-2010_12
ORD IDord-4ce0392fe6b54029a3fd70e0b4596c40
Source noteuspto-grants-2010_12