HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluorobenzenesulfonyl chloride → 2-[[(2,6-difluorophenyl)sulfonyl]amino]-4-iodoBenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluorobenzenesulfonyl chloride | HCID 2734271 | — |
| Reactant | 2-Amino-4-iodo-benzoic acid | HCID 22724780 | — |
| Product | 2-[[(2,6-difluorophenyl)sulfonyl]amino]-4-iodoBenzoic acid | HCID 68773651 | — |
Reaction Steps
2-Amino-4-iodo-benzoic acid was sulfonylated with 2,6-difluorobenzenesulfonyl chloride as in EXAMPLE 1, Part A. 1H NMR (500 MHz, CD3OD): 8.05 (d, J=1.6, 1H), 7.72 (d, J=8.4, 1H), 7.68-7.60 (m, 1H), 7.48 (dd, J=8.4, 1.6, 1H), 7.16-7.09 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855292B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-e07034c3393449919f673547fbbf5525 |
| Source note | uspto-grants-2010_12 |