HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluorobenzenesulfonyl chloride → HCID 68768495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluorobenzenesulfonyl chloride | HCID 2734271 | — |
| Reactant | Methyl 2-Amino-4-bromobenzoate | HCID 17871390 | — |
| Product | HCID 68768495 | HCID 68768495 | — |
Reaction Steps
Methyl 2-amino-4-bromobenzoate was sulfonylated with 2,6-difluorobenzenesulfonyl chloride and hydrolyzed as in EXAMPLE 1, Part B. 1H NMR (400 MHz, acetone-d6): 11.65 (s, 1H), 8.02 (d, J=8.5, 1H), 7.93 (d, J=1.8, 1H), 7.74-7.82 (m, 1H), 7.38 (dd, J=8.5, 1.9, 1H), 7.28-7.23 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855292B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-27edef2e8f514dcfa23747d3c0ff74eb |
| Source note | uspto-grants-2010_12 |