Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | HCID 59597487 | HCID 59597487 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 178515199 | HCID 178515199 | 85% |
Reaction Steps
In a vial were added 4a, phenyl hydrazine and triethylamine. The vial was sealed and heated to 135° C. for 12 hours. The product was collected by filtration and was washed with methanol in 85% yield. 1H-NMR (DMSO-d6) δ (ppm): 7.18 (1H, dd, J=7.41, 7.14 Hz), 7.50 (3H, m), 8.26 (3H, m), 8.81 (1H, s). m/z 281.3 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07858614B2 |
|---|
| Source dataset | uspto-grants-2010_12 |
|---|
| ORD ID | ord-2095792d6d01423d8e2285f3643f32e6 |
|---|
| Source note | uspto-grants-2010_12 |
|---|
